反应条件
1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 20 °C / |Inert atmosphere
2: trifluoroacetic acid / dichloromethane / 20 °C
3: triethylamine; bis(trichloromethyl) carbonate / ethyl acetate / 2 h / |Reflux
View Scheme
参考文献
Cui, Huaqing; Carrero-Lerida, Juana; Silva, Ana P. G.; Whittingham, Jean L.; Brannigan, James A.; Ruiz-Perez, Luis M.; Read, Kevin D.; Wilson, Keith S.; Gonzalez-Pacanowska, Dolores; Gilbert, Ian H.
Journal of Medicinal Chemistry, 2012 , vol. 55, # 24 p. 10948 - 10957
