1: 98 percent / H2 / 10percent Pd/C / ethyl acetate / 5 h / 2585.7 Torr / Ambient temperature 2: 89 percent / ammonium acetate, acetic acid / toluene / Heating 3: ethanol; H2O / 5 h / Heating 4: acetic acid, hydrochloric acid, H2O / 84 h / Heating View Scheme

hydrogen; palladium on activated charcoal in ethyl acetate P=2585.7 Torr; 5 h; Ambient temperature;

1: 98 percent / H2 / 10percent Pd/C / ethyl acetate / 5 h / 2585.7 Torr / Ambient temperature 2: 89 percent / ammonium acetate, acetic acid / toluene / Heating 3: ethanol; H2O / 5 h / Heating 4: acetic acid, hydrochloric acid, H2O / 84 h / Heating 5: 89 percent / acetic anhydride / 4 h / Heating View Scheme

1: 98 percent / H2 / 10percent Pd/C / ethyl acetate / 5 h / 2585.7 Torr / Ambient temperature 2: 89 percent / ammonium acetate, acetic acid / toluene / Heating 3: ethanol; H2O / 5 h / Heating 4: acetic acid, hydrochloric acid, H2O / 84 h / Heating 5: 89 percent / acetic anhydride / 4 h / Heating 6: Heating 7: LiAlH4 / diethyl ether / 3 h View Scheme

1: 98 percent / H2 / 10percent Pd/C / ethyl acetate / 5 h / 2585.7 Torr / Ambient temperature 2: 89 percent / ammonium acetate, acetic acid / toluene / Heating 3: ethanol; H2O / 5 h / Heating 4: acetic acid, hydrochloric acid, H2O / 84 h / Heating 5: 89 percent / acetic anhydride / 4 h / Heating 6: Heating 7: LiAlH4 / diethyl ether / 3 h View Scheme

1: 98 percent / H2 / 10percent Pd/C / ethyl acetate / 5 h / 2585.7 Torr / Ambient temperature 2: 89 percent / ammonium acetate, acetic acid / toluene / Heating 3: ethanol; H2O / 5 h / Heating 4: acetic acid, hydrochloric acid, H2O / 84 h / Heating 5: 89 percent / acetic anhydride / 4 h / Heating 6: 100 percent / Heating 7: 95 percent / LiAlH4 / diethyl ether / 3 h View Scheme

sulfuric acid in benzene 10 h; Heating;

1: 98 percent / H2 / 10percent Pd/C / ethyl acetate / 5 h / 2585.7 Torr / Ambient temperature 2: 89 percent / ammonium acetate, acetic acid / toluene / Heating View Scheme

1: 98 percent / H2 / 10percent Pd/C / ethyl acetate / 5 h / 2585.7 Torr / Ambient temperature 2: 89 percent / ammonium acetate, acetic acid / toluene / Heating 3: ethanol; H2O / 5 h / Heating 4: acetic acid, hydrochloric acid, H2O / 84 h / Heating 5: 89 percent / acetic anhydride / 4 h / Heating 6: Heating 7: LiAlH4 / diethyl ether / 3 h View Scheme