1-(4-甲氧基-苯基)-4-苯基-1,4-丁二酮合成路线 （共 26 条）
反应条件
carbon monoxide; triphenyl phosphite; bis(η3-allyl-μ-chloropalladium(II)) in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=100°C; P=7600 Torr; 20 h;
参考文献
Fujimura, Tsutomu; Aoki, Satoshi; Nakamura, Eiichi
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2809 - 2821
反应条件
carbon monoxide; triphenyl phosphite; palladium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=100°C; P=7600 Torr; 20 h;
参考文献
Aoki; Fujimura; Nakamura; Kuwajima
Tetrahedron Letters, 1989 , vol. 30, # 47 p. 6541 - 6544
反应条件
zinc(II) chloride in tetrahydrofuran
T=40°C; 4 h;
参考文献
Yasuda, Makoto; Tsuji, Shoki; Shigeyoshi, Yusuke; Baba, Akio
Journal of the American Chemical Society, 2002 , vol. 124, # 25 p. 7440 - 7447
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=100°C; P=15200 Torr;
参考文献
Aoki; Nakamura
Tetrahedron, 1991 , vol. 47, # 24 p. 3935 - 3946
反应条件
sodium carbonate; triethylamine; 3,4-dimethyl-5-(2-hydroxyethyl)-thiazolium iodide in ethanol
T=80°C; 8 h;
参考文献
Stetter, Hermann; Jonas, Friedrich
Chemische Berichte, 1981 , vol. 114, # 2 p. 564 - 580
反应条件
1: diiodomethane With diethylzinc; trifluoroacetic acid in dichloromethane
T=0°C; 0.5 h;
2: 1-(4'-methoxyphenyl)-3-phenylpropane-1,3-dione in dichloromethane
T=20°C; 5 h;
参考文献
Xue, Song; Li, Le-Zhen; Liu, Yong-Kang; Guo, Qing-Xiang
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 215 - 218
反应条件
ZnCl2*Et3N*t-BuOH in benzene
T=20°C; Condensation; 168 h;
参考文献
Nevar; Kel'in; Kulinkovich
Synthesis, 2000 , # 9 p. 1259 - 1262
反应条件
1: 5-Iodo-pentanoic acid ethyl ester With chloro-trimethyl-silane; ethylene dibromide; zinc in tetrahydrofuran
T=35°C; 20 h;
2: PhSBz With bis(acetylacetonate)nickel(II) in tetrahydrofuran; toluene
T=20°C; 20 h;
参考文献
Shimizu, Toshiaki; Seki, Masahiko
Tetrahedron Letters, 2002 , vol. 43, # 6 p. 1039 - 1042
参考文献
Matsumoto, Takahiro; Katayama, Nozomi; Mabuchi, Hiroshi
Patent: US2003/144338 A1, 2003 ;
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O; potassium carbonate; triethylamine in acetonitrile
T=20°C; 14 h; Schlenk techniqueIrradiation;
参考文献
Xuan, Jun; Feng, Zhu-Jia; Chen, Jia-Rong; Lu, Liang-Qiu; Xiao, Wen-Jing
Chemistry - A European Journal, 2014 , vol. 20, # 11 p. 3045 - 3049
