3-甲氧基-3,7-二甲基辛-1,6-二烯合成路线 （共 10 条）
反应条件
1: 3,7-Dimethyl-1.6-octadien-3-ol With sodium hydride in N,N-dimethyl-formamide
T=0°C; 0.5 h; Inert atmosphere;
2: methyl iodide in N,N-dimethyl-formamide
2 h; Inert atmosphere;
参考文献
Justicia, Jose; Jimenez, Tania; Miguel, Delia; Contreras-Montoya, Rafael; Chahboun, Rachid; Alvarez-Manzaneda, Enrique; Collado-Sanz, Daniel; Cardenas, Diego J.; Cuerva, Juan M.
Chemistry - A European Journal, 2013 , vol. 19, # 43 p. 14484 - 14495
反应条件
palladium dichloride
T=60°C; 20 h;
参考文献
Ito, Satoru; Matsumoto, Masakatsu
Synthetic Communications, 1982 , vol. 12, # 10 p. 807 - 812
反应条件
ruthenium trichloride
参考文献
Ito, Satoru; Matsumoto, Masakatsu
Synthetic Communications, 1982 , vol. 12, # 10 p. 807 - 812
反应条件
ruthenium trichloride
参考文献
Ito, Satoru; Matsumoto, Masakatsu
Synthetic Communications, 1982 , vol. 12, # 10 p. 807 - 812
反应条件
ruthenium trichloride
参考文献
Ito, Satoru; Matsumoto, Masakatsu
Synthetic Communications, 1982 , vol. 12, # 10 p. 807 - 812
反应条件
Lindlar's catalyst; Petroleum ether
Hydrogenation;
参考文献
Hoffmann-La Roche
Patent: US2841620 , 1956 ;
反应条件
1: liquid ammonia; toluene / und Einleiten von Brommethan in das vom Ammoniak befreite Reaktionsgemisch
2: Lindlar-catalyst; petroleum ether / Hydrogenation
View Scheme
参考文献
Hoffmann-La Roche
Patent: US2841620 , 1956 ;
反应条件
(i) TsNHNH2, (ii) /BRN= 1098229/, NaBH4; Multistep reaction;
参考文献
Grandi,R. et al.
Journal of Organic Chemistry, 1976 , vol. 41, # 10 p. 1755 - 1758
反应条件
tetraethylammonium p-toluenesulfonate
electrolysis, undivided cell, carbon rod electrodes; Yield given. Yields of byproduct given;
参考文献
Yoshida, Jun-ichi; Murata, Toshiki; Isoe, Sachihiko
Tetrahedron Letters, 1986 , vol. 27, # 29 p. 3373 - 3376
反应条件
hydrogenchloride
5 h; Irradiationother alkylmercaptoazoles, var solvents and temperatures; Product distribution;
参考文献
Iwasaki, Shigeo
Heterocycles, 1982 , vol. 17, p. 125 - 138
