2,2'-氧代双乙胺二盐酸盐合成路线 （共 7 条）
反应条件
hydrogenchloride; hydrazine hydrate 1.) methanol, 1 h, reflux; 2.) water, 1 h, reflux;
参考文献
Abajo, J. de; Campa, J. G. de la; Riande, E.; Garcia, J. M.; Jimeno, M. L.
Journal of Physical Chemistry, 1993 , vol. 97, # 33 p. 8669 - 8674
反应条件
hydrogenchloride in diethyl ether; water Cooling with ice;
参考文献
Link, Andreas; Heidler, Philipp; Kaiser, Marcel; Brun, Reto
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 9 p. 3665 - 3671
反应条件
1: With sodium hydroxide; triethylamine in methanol T=20°C; 2 h; 2: With chloroformic acid ethyl ester T=0 - 20°C; 2 h;
参考文献
Herges, Rainer; Dikmans, Anton; Jana, Umasish; Koehler, Felix; Jones, Peter G.; Dix, Ina; Fricke, Tom; Koenig, Burkhard
European Journal of Organic Chemistry, 2002 , # 17 p. 3004 - 3014
反应条件
sodium hydroxide in tetrahydrofuran; methanol T=20°C;
参考文献
Journal of Organic Chemistry, , vol. 72, # 7 p. 2289 - 2296
反应条件
sodium hydroxide in tetrahydrofuran; methanol T=20°C; 24 h;
参考文献
European Journal of Organic Chemistry, , # 17 p. 3004 - 3014
反应条件
ammonia in methanol; chloroform
参考文献
Cram, Donald J.; Ho, Siew Peng; Knobler, Carolyn B.; Maverick, Emily; Trueblood, Kenneth N.
Journal of the American Chemical Society, 1986 , vol. 108, # 11 p. 2989 - 2998
反应条件
sodium hydroxide in acetonitrile
T=20°C; 16 h;
参考文献
Herges, Rainer; Dikmans, Anton; Jana, Umasish; Koehler, Felix; Jones, Peter G.; Dix, Ina; Fricke, Tom; Koenig, Burkhard
European Journal of Organic Chemistry, 2002 , # 17 p. 3004 - 3014
