1,3-二甲基-2-碘苯合成路线 （共 73 条）
反应条件
[PdCl2(1,3-bis(diphenylphosphino)propane)]; sodium carbonate in N,N-dimethyl-formamide; 1,3,5-trimethyl-benzene T=60°C; P=2250.23 Torr; 18 h; Sealed tube;
参考文献
Organic Process Research and Development, , vol. 11, # 1 p. 39 - 43
反应条件
triethylsilane; carbon monoxide; C16H36Cl2P2Pd; sodium carbonate in N,N-dimethyl-formamide T=100°C; P=2250.23 Torr; 24 h; Inert atmosphereAutoclave; Reagent/catalyst; chemoselective reaction;
参考文献
Barnard, Christopher F.J.
Organic Process Research and Development, 2008 , vol. 12, # 4 p. 566 - 574
反应条件
C44H34Br2P2Pd; potassium carbonate in 1-methyl-pyrrolidin-2-one T=100°C; P=3750.38 Torr; 24 h; Inert atmosphereAutoclave; Reagent/catalyst; chemoselective reaction;
参考文献
Organic Process Research and Development, , vol. 12, # 4 p. 566 - 574
反应条件
in dimethyl sulfoxide Substitution; Irradiation;
参考文献
European Journal of Organic Chemistry, , # 14 p. 2663 - 2668
反应条件
1: With isopropylmagnesium chloride in tetrahydrofuran T=0°C; Inert atmosphere; 2: With methanol in tetrahydrofuran Kinetics; ConcentrationTime;
参考文献
Shi, Lei; Chu, Yuanyuan; Knochel, Paul; Mayr, Herbert
Organic Letters, 2012 , vol. 14, # 10 p. 2602 - 2605
反应条件
1: With isopropylmagnesium chloride in tetrahydrofuran T=0°C; Inert atmosphere; 2: With methanol in tetrahydrofuran Kinetics; ConcentrationTime;
参考文献
Shi, Lei; Chu, Yuanyuan; Knochel, Paul; Mayr, Herbert
Organic Letters, 2012 , vol. 14, # 10 p. 2602 - 2605
反应条件
1: With isopropylmagnesium chloride in tetrahydrofuran T=0°C; Inert atmosphere; 2: With methanol in tetrahydrofuran Kinetics; ConcentrationTime;
参考文献
Shi, Lei; Chu, Yuanyuan; Knochel, Paul; Mayr, Herbert
Organic Letters, 2012 , vol. 14, # 10 p. 2602 - 2605
反应条件
1: With isopropylmagnesium chloride in tetrahydrofuran T=0°C; Inert atmosphere; 2: With methanol in tetrahydrofuran Kinetics; ConcentrationTime;
参考文献
Shi, Lei; Chu, Yuanyuan; Knochel, Paul; Mayr, Herbert
Organic Letters, 2012 , vol. 14, # 10 p. 2602 - 2605
参考文献
Klages; Liecke
Journal fuer Praktische Chemie (Leipzig), 1900 , vol. <2> 61, p. 322
反应条件
CyPF-tBu; palladium diacetate; sodium t-butanolate in ethylene glycol dimethyl ether T=110°C; 8 h; Inert atmosphere;
参考文献
Fernandez-Rodriguez, Manuel A.; Hartwig, John F.
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1664 - 1672
