反应条件
1.1: n-BuLi / hexane; tetrahydrofuran / 0.67 h / -78 °C
1.2: 78 percent / tetrahydrofuran; hexane / 4 h
2.1: 100 percent / NaH / dimethylformamide / 6 h / 85 °C
3.1: 82 percent / 4 h / 240 °C
4.1: LiAlH4 / tetrahydrofuran / 12 h / Heating
4.2: 71 percent / aq. HCl / tetrahydrofuran
5.1: 100 percent / Et3N / petroleum ether / 60 h / 0 - 20 °C
6.1: 100 percent / trifluoroacetic acid / 2.5 h / 0 °C
View Scheme
参考文献
Nishide, Kiyoharu; Ohsugi, Shin-Ichi; Miyamoto, Tetsuo; Kumar, Kamal; Node, Manabu
Monatshefte fur Chemie, 2004 , vol. 135, # 2 p. 189 - 200
