N-苄氧羰基-D-丝氨酸合成路线 （共 10 条）
反应条件
sodium hydrogencarbonate in tetrahydrofuran; water T=20°C; 12 h;
参考文献
Wu, Ju; Ma, Bing; Wang, Yuehui; Zhang, Yue; Yan, Shenghu; Castle, Steven L.
Tetrahedron Letters, 2014 , vol. 55, # 19 p. 3114 - 3116
反应条件
sodium hydroxide; benzyl chloroformate
参考文献
Journal of the American Chemical Society, , vol. 76, p. 2887,2890
反应条件
citrate buffer; dl-cysteine hydrochloride; papain T=50°C; 24 h;
参考文献
Synthetic Communications, , vol. 18, # 4 p. 441 - 444
反应条件
resolved on CSP cellulose tris(3,5-dimethylphenylcarbamate) by chiral HPLC;
参考文献
Chemistry Letters, , p. 1125 - 1128
反应条件
1.1: 4-methylmorpholine / tetrahydrofuran / 0.03 h / -78 °C 1.2: isobutyl chloroformate / tetrahydrofuran / 0.03 h 1.3: 65 percent / tetrahydrofuran / -78 - 20 °C 2.1: 90 percent / Ag2O / acetonitrile / 20 °C View Scheme
参考文献
King, Amber M.; Salome, Christophe; Dinsmore, Jason; Salome-Grosjean, Elise; De Ryck, Marc; Kaminski, Rafal; Valade, Anne; Kohn, Harold
Journal of Medicinal Chemistry, 2011 , vol. 54, # 13 p. 4815 - 4830
反应条件
MeO2CN=NCO2Me; triphenylphosphine in tetrahydrofuran T=20°C; 2.5 h;
参考文献
Arnold; Kalantar; Vederas
Journal of the American Chemical Society, 1985 , vol. 107, # 24 p. 7105 - 7109
参考文献
Scheurer, Andreas; Mosset, Paul; Bauer, Walter; Saalfrank, Rolf W.
European Journal of Organic Chemistry, 2001 , # 16 p. 3067 - 3074
反应条件
1: 60 percent / Ph3P, dimethyl azodicarboxylate / tetrahydrofuran / 2.5 h / 20 °C 2: 88 percent / methanol; tetrahydrofuran / 0.42 h / 22 °C View Scheme
参考文献
Arnold; Kalantar; Vederas
Journal of the American Chemical Society, 1985 , vol. 107, # 24 p. 7105 - 7109
反应条件
1: 60 percent / Ph3P, dimethyl azodicarboxylate / tetrahydrofuran / 2.5 h / 20 °C 2: 12 percent / methanol; tetrahydrofuran / 0.42 h / 22 °C View Scheme
参考文献
Arnold; Kalantar; Vederas
Journal of the American Chemical Society, 1985 , vol. 107, # 24 p. 7105 - 7109
参考文献
Pfizer Inc.
Patent: US4454328 A1, 1984 ;
