7-氯-2,3-二氢吡咯并[2,1-b]喹唑啉-9(1h)-酮合成路线 （共 7 条）
反应条件
acetic acid; sodium iodide
3 h; Heating;
参考文献
Kamal, Ahmed; Ramana, A. Venkata; Reddy, K. Srinivasa; Ramana, K. Venkata; Hari Babu; Prasad, B. Rajendra
Tetrahedron Letters, 2004 , vol. 45, # 44 p. 8187 - 8190
反应条件
thionyl chloride in benzene
参考文献
Farmitalia Carlo Erba S.p.A.
Patent: US4428952 A1, 1984 ;
反应条件
thionyl chloride in benzene
4 h; Reflux;
参考文献
Jahng, Katherine Chae; Kim, Seung Ill; Kim, Dong Hyeon; Seo, Chang Seob; Son, Jong-Keun; Lee, Seung Ho; Lee, Eung Seok; Jahng, Yurngdong
Chemical and Pharmaceutical Bulletin, 2008 , vol. 56, # 4 p. 607 - 609
反应条件
phosphorous pentoxide in m-xylene
3 h; Reflux;
参考文献
Ojo, Babatunde; Chowdhury, Bejoy K.
Synthetic Communications, 2012 , vol. 42, # 7 p. 1002 - 1009
反应条件
1: Et3N / tetrahydrofuran / 20 °C
2: 94 percent / sodium iodide; acetic acid / 3 h / Heating
View Scheme
参考文献
Kamal, Ahmed; Ramana, A. Venkata; Reddy, K. Srinivasa; Ramana, K. Venkata; Hari Babu; Prasad, B. Rajendra
Tetrahedron Letters, 2004 , vol. 45, # 44 p. 8187 - 8190
反应条件
1: sulfuryl dichloride / diethyl ether / 20 °C / Cooling
2: phosphorous pentoxide / m-xylene / 3 h / Reflux
View Scheme
参考文献
Ojo, Babatunde; Chowdhury, Bejoy K.
Synthetic Communications, 2012 , vol. 42, # 7 p. 1002 - 1009
反应条件
Amberlyst A-26 Br3(-) form in tetrahydrofuran
T=20°C;
参考文献
Kamal, Ahmed; Devaiah; Shankaraiah; Laxma Reddy
Synlett, 2006 , # 16 p. 2609 - 2612
