反应条件
1: N-(2-hydroxyethyl)-ethylamine With sodium hydride in DMF (N,N-dimethyl-formamide)
T=-5 - 45°C; 1.16667 h;
2: 4-fluoro-nitro-benzene in DMF (N,N-dimethyl-formamide)
T=-10 - 20°C; 1.83333 h;
参考文献
Chu, Xin-Jie; Ding, Qingjie; Jiang, Nan; Kim, Kyungjin; Lovey, Allen John; McComas, Warren William; Mullin JR., John Guilfoyle; Tilley, Jefferson Wright
Patent: US2004/6058 A1, 2004 ;
Location in patent: Page/Page column 93 ;
US 20040006058 A1
