反应条件
1: 1.) n-BuLi / 1.) THF, -78 deg C, 50 min, 2.) THF, -78 deg C, 2h
2: m-chloroperoxybenzoic acid / CH2Cl2 / 0.25 h / -5 °C
3: CCl4 / 6 h / Heating
View Scheme
参考文献
Clinet, J. C.; Balavoine, G.
Tetrahedron Letters, 1987 , vol. 28, # 45 p. 5509 - 5512