4'-氨基苯并-15-冠-5-醚合成路线 （共 10 条）
反应条件
hydrazine hydrate; palladium on activated charcoal in 1,4-dioxane
参考文献
Yang, Jye-Shane; Hwang, Chung-Yu; Chen, Mon-Yao
Tetrahedron Letters, 2007 , vol. 48, # 17 p. 3097 - 3102
参考文献
Acta Chimica Academiae Scientiarum Hungaricae, , vol. 110, # 1 p. 25 - 28
反应条件
1: 52 percent / NaOH / butan-1-ol 2: 98 percent / aq. HNO3; CH3COOH / CHCl3 3: 100 percent / N2H4*nH2O / Pd/C / dioxane View Scheme
参考文献
Tetrahedron Letters, , vol. 48, # 17 p. 3097 - 3102
反应条件
1: 52 percent / NaOH / butan-1-ol 2: 98 percent / aq. HNO3; CH3COOH / CHCl3 3: 100 percent / N2H4*nH2O / Pd/C / dioxane View Scheme
参考文献
Tetrahedron Letters, , vol. 48, # 17 p. 3097 - 3102
反应条件
in chlorobenzene Heating;
参考文献
Acta Chimica Academiae Scientiarum Hungaricae, , vol. 110, # 1 p. 25 - 28
Liebigs Annalen der Chemie, , p. 349 - 354
参考文献
Toeke, Laszlo; Bitter, Istvan; Agai, Bela; Csongor, Eva; Toth, Klara; et al.
Liebigs Annalen der Chemie, 1988 , p. 349 - 354
反应条件
1: 2) nitric acid / 1) glacial acetic acid, 80 deg C, 1 h, 2) 60 deg C
2: 70 percent / 18percent aq. HCl / Heating
3: 94 percent / chlorobenzene / Heating
View Scheme
参考文献
Agai, B.; Bitter, I.; Csongor, E.; Toeke, L.
Acta Chimica Academiae Scientiarum Hungaricae, 1982 , vol. 110, # 1 p. 25 - 28
反应条件
1: 87 percent / chlorobenzene / Heating
2: CH2Cl2 / 2 h / Ambient temperature
View Scheme
参考文献
Agai, B.; Bitter, I.; Csongor, E.; Toeke, L.
Acta Chimica Academiae Scientiarum Hungaricae, 1982 , vol. 110, # 1 p. 25 - 28
反应条件
1: 87 percent / chlorobenzene / Heating
2: CH2Cl2 / 2 h / Ambient temperature
View Scheme
参考文献
Agai, B.; Bitter, I.; Csongor, E.; Toeke, L.
Acta Chimica Academiae Scientiarum Hungaricae, 1982 , vol. 110, # 1 p. 25 - 28
反应条件
1: 2) nitric acid / 1) glacial acetic acid, 80 deg C, 1 h, 2) 60 deg C
2: 70 percent / 18percent aq. HCl / Heating
3: 94 percent / chlorobenzene / Heating
4: CH2Cl2 / 2 h / Ambient temperature
View Scheme
参考文献
Agai, B.; Bitter, I.; Csongor, E.; Toeke, L.
Acta Chimica Academiae Scientiarum Hungaricae, 1982 , vol. 110, # 1 p. 25 - 28
