1: 75 percent / sodium carbonate, potassium permanganate / H2O / 1.) 0 deg C, 2 h, 2.) room temperature, 12 h 2: 99 percent / oxalyl chloride, pyridine / CH2Cl2 / 4 h / Ambient temperature 3: 80 percent / pyridine / 18 h / Ambient temperature View Scheme
参考文献
Haines, Alan H.; Hodgkisson, Ian; Smith, Christopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 311 - 318
Gunter, Maxwell J.; Johnston, Martin R.; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 8 p. 1009 - 1018