4'-甲酰苯并-18-冠-6-醚合成路线 （共 8 条）
反应条件
1: 3,4-dihydroxy-benzaldehyde With potassium carbonate in N,N-dimethyl-formamide T=80°C; 0.5 h; 2: pentaethylene glycol di-p-toluenesulphonate in N,N-dimethyl-formamide T=80°C; 20 h;
参考文献
D'Souza, Francis; Chitta, Raghu; Gadde, Suresh; Zandler, Melvin E.; Sandanayaka, Atula S. D.; Araki, Yasuyuki; Ito, Osamu
Chemical Communications, 2005 , # 10 p. 1279 - 1281
反应条件
sodium hydroxide in butan-1-ol 48 h; Heating;
参考文献
Lindsten, Goeran; Wennerstroem, Olof; Thulin, Bengt
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 7 p. 545 - 554
反应条件
trifluoroacetic acid T=85 - 90°C; 24 h;
参考文献
Wada, Fumio; Hirayama, Hiroshi; Namiki, Hiroshi
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 5 p. 1473 - 1474
参考文献
Kryatova, Olga P.; Kolchinski, Alexander G.; Rybak-Akimova, Elena V.
Tetrahedron, 2003 , vol. 59, # 2 p. 231 - 239
反应条件
1,7-heptanediammonium diperchlorate; oxygen in acetonitrile 2 h; UV-irradiation; stereoselective reaction;
参考文献
Russian Chemical Bulletin, , vol. 58, # 1 p. 108 - 114
反应条件
hydrogenchloride; n-butyllithium 1.) ether-THF, -60 deg C; Yield given. Multistep reaction;
参考文献
Russian Chemical Bulletin, , vol. 42, # 5 p. 960 - 961
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 5 p. 996
反应条件
n-butyllithium 1) Et2O, THF, hexane, -60 deg C, 4.0 h; 2) DMF, Et2O, THF, hexane, -60 deg C, 1.2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Russian Chemical Bulletin, , vol. 44, # 1 p. 116 - 123
Izvestiya Akademi Nauk, Seriya Khimicheskaya, , # 1 p. 121 - 128
反应条件
n-butyllithium 1) Et2O, THF, hexane, -60 deg C, 4.0 h; 2) Et2O, THF, hexane, -60 deg C, 1.2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Russian Chemical Bulletin, , vol. 44, # 1 p. 116 - 123
Izvestiya Akademi Nauk, Seriya Khimicheskaya, , # 1 p. 121 - 128
