[(E)-十八碳-9-烯酰基](E)-十八碳-9-烯酸酯合成路线 (共 9 条)
参考文献
Harris; Marshall; Lee; Siegel; Mcneilly; Yew; Nietupski; Nichols; Cherry; Wan; Jiang; Lane; Rowe; Scheule; Smith; Cheng
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 109, # 1-4 p. 289 - 292
参考文献
Israel Journal of Chemistry, , vol. 3, p. 120p
反应条件
octadec-9c-enoic acid lt;tetraethylammonium saltgt;
参考文献
Cubero Robles,E.; de Iongh,H.
Recueil des Travaux Chimiques des Pays-Bas, 1967 , vol. 86, p. 762 - 764
反应条件
1: 66 percent 2: 80 percent View Scheme
参考文献
Harris; Marshall; Lee; Siegel; Mcneilly; Yew; Nietupski; Nichols; Cherry; Wan; Jiang; Lane; Rowe; Scheule; Smith; Cheng
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 109, # 1-4 p. 289 - 292
反应条件
boron trifluoride diethyl etherate in chloroform T=61°C; Acylation; 4 h;
参考文献
Tetrahedron, , vol. 56, # 49 p. 9697 - 9703
反应条件
trimethylsilyl bromide; tetrabutylammomium bromide in chloroform 2 h; Heating;
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 23 p. 3787 - 3800
反应条件
1: 66 percent 2: 80 percent 3: 90 percent / PLD View Scheme
参考文献
Harris; Marshall; Lee; Siegel; Mcneilly; Yew; Nietupski; Nichols; Cherry; Wan; Jiang; Lane; Rowe; Scheule; Smith; Cheng
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 109, # 1-4 p. 289 - 292
反应条件
hydrogen; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=80°C; Catalytic hydrogenation; P=22501.8 Torr; 24 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 72, # 3 p. 573 - 580
反应条件
osmium(VIII) oxide; potassium hexacyanoferrate(III) in water Title compound not separated from byproducts;
参考文献
Angewandte Chemie, International Edition, , vol. 40, # 1 p. 199 - 202
Angewandte Chemie, , vol. 113, p. 205 - 208