1-(2-氯苯基)-2-(1H-1,2,4-噻唑-1-基)-乙酮合成路线 （共 4 条）
反应条件
sulfuric acid; sodium nitrite in water
T=0 - 20°C; 2 h;
参考文献
Krimer, M. Z.; Tashi, B. P.; Roitburd, G. V.; Shtirkov, I. M.; Manaev, S. A.; et al.
Doklady Chemistry, 1989 , vol. 308, # 4-6 p. 299 - 301
Dokl. Akad. Nauk SSSR Ser. Khim., 1989 , vol. 308, # 5 p. 1155 - 1158
反应条件
1: Br2; acetic acid
2: anhydrous potassium carbonate / CHCl3 / Heating
View Scheme
参考文献
Ling, Shao; Xin, Zhou; Qing, Zhang; Jian-Bing, Liu; Zhong, Jin; Jian-Xin, Fang
Synthetic Communications, 2007 , vol. 37, # 2 p. 199 - 207
反应条件
1: acetonitrile / 80 - 85 °C
2: conc. H2SO4, NaNO2 / H2O / 2 h / 0 - 20 °C
View Scheme
参考文献
Krimer, M. Z.; Tashi, B. P.; Roitburd, G. V.; Shtirkov, I. M.; Manaev, S. A.; et al.
Doklady Chemistry, 1989 , vol. 308, # 4-6 p. 299 - 301
Dokl. Akad. Nauk SSSR Ser. Khim., 1989 , vol. 308, # 5 p. 1155 - 1158
反应条件
potassium carbonate in chloroform
Heating;
参考文献
Ling, Shao; Xin, Zhou; Qing, Zhang; Jian-Bing, Liu; Zhong, Jin; Jian-Xin, Fang
Synthetic Communications, 2007 , vol. 37, # 2 p. 199 - 207
