N-甲氧基-N,1-二甲基环丙烷甲酰胺合成路线 (共 1 条)
反应条件
1: 1-methylcyclopropane-1-carboxylic acid With oxalyl dichloride in diethyl ether
T=0 - 20°C; 11 h; Inert atmosphere;
2: O,N-dimethyl-hydroxylamine hydrochloride With pyridine in diethyl ether; chloroform
T=0 - 20°C; 23 h; Inert atmosphere;
参考文献
Shintani, Ryo; Nakatsu, Hiroki; Takatsu, Keishi; Hayashi, Tamio
Chemistry - A European Journal, 2009 , vol. 15, # 35 p. 8692 - 8694