2-氨基-3,5-二溴苯甲酸合成路线 （共 65 条）
反应条件
Verkochen der Diazoloesung mit Alkohol.Diazotization;
参考文献
Bogert; Hand
Journal of the American Chemical Society, 1903 , vol. 25, p. 939
反应条件
Erwaermen der Diazoloesung mit Alkohol und Kupfersulfat.Diazotization;
参考文献
Elion
Recueil des Travaux Chimiques des Pays-Bas, 1923 , vol. 42, p. 151,153,164,168
Recueil des Travaux Chimiques des Pays-Bas, 1924 , vol. 43, p. 867
参考文献
Rosanoff; Prager
Journal of the American Chemical Society, 1908 , vol. 30, p. 1904
Zeitschrift fuer Physikalische Chemie, Stoechiometrie und Verwandtschaftslehre, 1909 , vol. 66, p. 286
反应条件
1: 3,5-dibromo-anthranilic acid With 4-(N,N-dimethlyamino)pyridine; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide in dichloromethane 1 h; 2: N-cyclohexyl-N-methylamine in dichloromethane 1 h;
参考文献
Larsen, Uffe S.; Begtrup, Mikael; Martiny, Lars
Journal of Labelled Compounds and Radiopharmaceuticals, 2005 , vol. 48, # 6 p. 429 - 434
参考文献
Chemische Berichte, , vol. 44, p. 427
Journal of the Chemical Society, , vol. 111, p. 47
反应条件
1: pyridine / 1) 0 to 5 deg C, 1h, 2) RT, overnight 2: 75 percent / pyridine / Heating 3: 1) EtOH, 1h, reflux, 2) 12h, reflux View Scheme
参考文献
Kulkarni; Bishnoi
Journal of the Indian Chemical Society, 1990 , vol. 67, # 10 p. 852 - 854
反应条件
phosphorus pentachloride; benzene anschliessend Behandeln mit Ammoniumcarbonat;
参考文献
Sheibley
Journal of Organic Chemistry, 1947 , vol. 12, p. 743,747
参考文献
Sheibley
Journal of Organic Chemistry, 1947 , vol. 12, p. 743,747
反应条件
1: 1 h / Heating
2: piperidine / ethanol / 10 h / Heating
View Scheme
参考文献
Kassab, R. R.; El-Hashash, M. A.; Ahmad, I. GH.
Egyptian Journal of Chemistry, 2003 , vol. 46, # 3 p. 487 - 500
反应条件
pyridine
0.5 h; Reflux;
参考文献
Saravanan, Govindaraj; Alagarsamy, Veerachamy; Prakash, Chinnasamy Rajaram
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 9 p. 3072 - 3078
