2,6-二甲基-2,5-庚二烯合成路线 （共 18 条）
反应条件
dichloro bis(acetonitrile) palladium(II); triphenylphosphine in chloroform-d1
T=65°C; 48 h;
参考文献
Sheffy; Godschalx; Stille
Journal of the American Chemical Society, 1984 , vol. 106, # 17 p. 4833 - 4840
反应条件
pyridine; thionyl chloride in benzene
T=0 - 20°C;
参考文献
Carless, Howard A.J.; Batten, Richard J.
Tetrahedron Letters, 1982 , vol. 23, # 45 p. 4735 - 4738
反应条件
γ-Al2O3
T=200°C; flow reactor;
参考文献
Molnar, Arpad; Bartok, Mihaly
Tetrahedron, 1987 , vol. 43, # 1 p. 131 - 142
参考文献
Bateman et al.
Journal of the Chemical Society, 1952 , p. 1714,1717
参考文献
Bateman et al.
Journal of the Chemical Society, 1952 , p. 1714,1717
反应条件
1: 55 percent / 10 percent sulphuric acid
2: 39 percent Chromat. / γ-Al2O3 / 200 °C / flow reactor
View Scheme
参考文献
Molnar, Arpad; Bartok, Mihaly
Tetrahedron, 1987 , vol. 43, # 1 p. 131 - 142
反应条件
1: pyridine; phosphorus (III)-chloride
2: pyridine / 140 °C
View Scheme
参考文献
Bateman et al.
Journal of the Chemical Society, 1952 , p. 1714,1717
反应条件
1: benzene
2: (i) PhLi, Et2O, (ii) /BRN= 635680/
View Scheme
参考文献
Ansell,M.F.; Thomas,D.A.
Journal of the Chemical Society, 1961 , p. 539 - 542
参考文献
Bateman et al.
Journal of the Chemical Society, 1952 , p. 1714,1717
反应条件
tetrabutylammonium dibromocuprate(I); lithium
1.) ethyl ether, -15 deg C, 2 h, 2.) ethyl ether, -70 deg C; Yield given. Multistep reaction;
参考文献
Baeckstroem, Peter; Bjoerkling, Fredrik; Hoegberg, Hans-Erik; Norin, Torbjoern
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 9 p. 779 - 782
