2,6-二甲基-2,5-庚二烯合成路线 （共 18 条）
反应条件
(i) Et2O, (ii) Li, NH3; Multistep reaction;
参考文献
Zilenovski,J.S.R.; Hall,S.S.
Journal of Organic Chemistry, 1979 , vol. 44, p. 1159 - 1161
反应条件
γ-Al2O3
T=350°C; variation of temperatures; Product distribution;
参考文献
Molnar, Arpad; Bartok, Mihaly
Tetrahedron, 1987 , vol. 43, # 1 p. 131 - 142
反应条件
(i), (ii) (dehydration); Multistep reaction;
参考文献
Biot,J.M.; Verzele,M.
Bulletin des Societes Chimiques Belges, 1977 , vol. 86, p. 41 - 46
反应条件
(i) PhLi, Et2O, (ii) /BRN= 635680/; Multistep reaction;
参考文献
Ansell,M.F.; Thomas,D.A.
Journal of the Chemical Society, 1961 , p. 539 - 542
反应条件
tetrabutylammomium bromide; oxygen; rose bengal; tetra-N-butylammonium borohydride in chloroform
1.75 h; Irradiation;
参考文献
Baeckstroem, Peter; Bjoerkling, Fredrik; Hoegberg, Hans-Erik; Norin, Torbjoern
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 9 p. 779 - 782
反应条件
1: 21 percent / tetraphenylporphine, O2 / CH2Cl2 / 2 h / -50 °C
2: triphenylphosphine
View Scheme
参考文献
Carless, Howard A.J.; Batten, Richard J.
Tetrahedron Letters, 1982 , vol. 23, # 45 p. 4735 - 4738
反应条件
tetrabutylammomium bromide; oxygen; rose bengal; tetra-N-butylammonium borohydride in chloroform
1.75 h; Irradiation;
参考文献
Baeckstroem, Peter; Bjoerkling, Fredrik; Hoegberg, Hans-Erik; Norin, Torbjoern
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 9 p. 779 - 782
反应条件
1: 13 percent / tetraphenylporphine, O2 / CH2Cl2 / 2 h / -50 °C
2: triphenylphosphine
View Scheme
参考文献
Carless, Howard A.J.; Batten, Richard J.
Tetrahedron Letters, 1982 , vol. 23, # 45 p. 4735 - 4738
