1: chlorosulfonic acid / neat (no solvent) / 0.17 h / 20 - 100 °C 2: sulfuric acid; potassium nitrate / 0 - 20 °C / |Large scale 3: hydrogen; 5 palladium on charcoal / tetrahydrofuran; ethanol / 4 h / 25 °C / 2311.54 Torr / |Large scale View Scheme
参考文献
Bellizzi, Mary E.; Bhatia, Ashok V.; Cullen, Steven C.; Gandarilla, Jorge; Kruger, Albert W.; Welch, Dennie S.
Organic Process Research and Development, 2014 , vol. 18, # 2 p. 303 - 309
1: chlorosulfonic acid / neat (no solvent) / 0.17 h / 20 - 100 °C 2: sulfuric acid; potassium nitrate / 0 - 20 °C / |Large scale View Scheme
参考文献
Bellizzi, Mary E.; Bhatia, Ashok V.; Cullen, Steven C.; Gandarilla, Jorge; Kruger, Albert W.; Welch, Dennie S.
Organic Process Research and Development, 2014 , vol. 18, # 2 p. 303 - 309
