1,1':2',1''-三联苯-3'-醇合成路线 （共 12 条）
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in 1-methyl-pyrrolidin-2-one
T=90°C; 15 h; Molecular sieveInert atmosphere; regioselective reaction;
参考文献
Imahori, Tatsushi; Tokuda, Toru; Taguchi, Tatsuya; Takahata, Hiroki
Organic Letters, 2012 , vol. 14, # 4 p. 1172 - 1175
反应条件
sulfuric acid in diethyl ether
1 h;
参考文献
Alonso; Yus
Tetrahedron, 1992 , vol. 48, # 13 p. 2709 - 2714
反应条件
in tetrahydrofuran
-78 deg C up to 20 deg C over 6 h;
参考文献
Alonso; Yus
Tetrahedron, 1992 , vol. 48, # 13 p. 2709 - 2714
反应条件
palladium diacetate; diisopropylamine in water
T=100°C; Suzuki-Miyaura Coupling;
参考文献
Luo, Shuang; Luo, Fei-Xian; Zhang, Xi-Sha; Shi, Zhang-Jie
Angewandte Chemie - International Edition, 2013 , vol. 52, # 40 p. 10598 - 10601
Angew. Chem., 2013 , vol. 125, # 40 p. 10792 - 10795,4
反应条件
platinum on activated charcoal
参考文献
Levin, Petr. P.; Khudyakov, Igor V.; Kuz'min, Vladimir A.; Hageman, Hendrik J.; Jonge, Cornelis R. H. I. de
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1237 - 1239
反应条件
1: Al / 1.) 250 deg C; 2.) 60 deg C, 2 h
2: 68 percent / Pt/C
View Scheme
参考文献
Levin, Petr. P.; Khudyakov, Igor V.; Kuz'min, Vladimir A.; Hageman, Hendrik J.; Jonge, Cornelis R. H. I. de
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1237 - 1239
反应条件
1: Al / 1.) 250 deg C; 2.) 60 deg C, 2 h
2: 68 percent / Pt/C
View Scheme
参考文献
Levin, Petr. P.; Khudyakov, Igor V.; Kuz'min, Vladimir A.; Hageman, Hendrik J.; Jonge, Cornelis R. H. I. de
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1237 - 1239
参考文献
Luettringhaus; Wagner-v. Saeaef
Justus Liebigs Annalen der Chemie, 1947 , vol. 557, p. 25,43
反应条件
in ethanol
8 h; Ambient temperatureIrradiation;
参考文献
Haga, Naoki; Takayanagi, Hiroaki
Journal of Organic Chemistry, 1996 , vol. 61, # 2 p. 735 - 745
反应条件
hydrogenchloride; acetic acid
Diazotization.Eintragen in Wasser;
参考文献
Monsanto Chem. Co.
Patent: US2267155 , 1940 ;
Full Text Show Details
Luettringhaus; Wagner-v. Saeaef
Justus Liebigs Annalen der Chemie, 1947 , vol. 557, p. 25,43
