双(三甲基硅基环戊二烯)二氯化锆合成路线 (共 13 条)
反应条件
aq. HCl in diethyl ether N2-atmosphere; 25°C;
参考文献
Journal of Organometallic Chemistry, , vol. 524, # 1-2 p. 49 - 61
反应条件
in neat (no solvent) CO (1 atm) was added to Zr complex;
参考文献
Canadian Journal of Chemistry, , vol. 83, # 4 p. 286 - 295
反应条件
methylaluminoxane in benzene-d6 under Ar, standard Schlenk techniques; solid dichloride Zr complex mixedwith 1 equiv. of Cp2ZrClMe; dissolved in benzene-d6; a minute amt. of s olid methylaluminoxane added; equil. reached within several min; not isolated; monitored by (1)H NMR spectra;
参考文献
Weiser, Ulrich; Babushkin, Dimitrii; Brintzinger, Hans-Herbert
Organometallics, 2002 , vol. 21, p. 920 - 923