3-(2,4-二甲氧基苯基)-3-氧代丙酸乙酯合成路线 （共 3 条）
反应条件
1: anhydrous iron chloride; oxygen / 1,2-dichloro-ethane / 24 h / 100 °C 2: boron tribromide / dichloromethane / 0 - 20 °C / |Inert atmosphere 3: ethanol / |Reflux View Scheme
参考文献
Kshirsagar, Umesh A.; Parnes, Regev; Goldshtein, Hagit; Ofir, Rivka; Zarivach, Raz; Pappo, Doron
Chemistry - A European Journal, 2013 , vol. 19, # 40 p. 13575 - 13583
反应条件
sodium hydride in toluene; paraffin oil
2 h; Inert atmosphereReflux;
参考文献
Al-Rifai, Nafisah; Ruecker, Hannelore; Amslinger, Sabine
Chemistry - A European Journal, 2013 , vol. 19, # 45 p. 15384 - 15395
反应条件
1: anhydrous iron chloride; di-tert-butyl peroxide; [2,2']bipyridinyl / 1,2-dichloro-ethane / 12 h / 70 °C / |Inert atmosphere
2: boron tribromide / dichloromethane / 0 - 20 °C / |Inert atmosphere
3: ethanol / |Reflux
View Scheme
参考文献
Kshirsagar, Umesh A.; Parnes, Regev; Goldshtein, Hagit; Ofir, Rivka; Zarivach, Raz; Pappo, Doron
Chemistry - A European Journal, 2013 , vol. 19, # 40 p. 13575 - 13583
