2-溴-2,4-二甲氧基苯乙酮合成路线 （共 12 条）
反应条件
copper(ll) bromide in chloroform; ethyl acetate 10 h; Inert atmosphereReflux;
参考文献
Al-Rifai, Nafisah; Ruecker, Hannelore; Amslinger, Sabine
Chemistry - A European Journal, 2013 , vol. 19, # 45 p. 15384 - 15395
反应条件
AlCl3, aluminium chloride T=23°C; Friedel-Crafts Acylation; 1 h;
参考文献
Penning, Miriam; Christoffers, Jens
European Journal of Organic Chemistry, 2013 , # 2 p. 389 - 400
反应条件
diethyl ether; hydrogen bromide; zinc(II) chloride und Kochen des Reaktionsprodukts mit Wasser;
参考文献
Chemische Berichte, , vol. 55, p. 2981
反应条件
in ethanol 1 h; Reflux;
参考文献
TAIVEX THERAPEUTICS CORPORATION; HUANG, Yu-Ling; CHUANG, Shih-Hsien; LEE, Ying-Shuan Eda; HUANG, Jiann-Jyh; LAU, Johnson
Patent: WO2013/82324 A1, 2013 ;
Location in patent: Paragraph 00352 ;
反应条件
bromine in chloroform
参考文献
European Journal of Medicinal Chemistry, , vol. 65, p. 102 - 111
反应条件
hydrogenchloride; sodium hydrogencarbonate 1.) ethanol, 3 h, heating; 2.) 5 h, heating; Yield given. Multistep reaction;
参考文献
Liu, Maili; Farrant, R. Duncan; Glen, Robert C.; Lindon, John C.; Barraclough, Paul; Smith, Steven
Magnetic Resonance in Chemistry, 1991 , vol. 29, # 11 p. 1147 - 1151
反应条件
N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide
T=20°C; 2 h;
参考文献
Macmillan, Derek; Anderson, David W.
Organic Letters, 2004 , vol. 6, # 25 p. 4659 - 4662
反应条件
N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide
T=20°C; 2 h;
参考文献
Macmillan, Derek; Anderson, David W.
Organic Letters, 2004 , vol. 6, # 25 p. 4659 - 4662
反应条件
1: acetone / 0.17 h / Heating
2: 2N HBr / 1 h
View Scheme
参考文献
Andreani; Rambaldi; Bonazzi; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 3 p. 219 - 222
反应条件
1: acetone / 0.17 h / Heating
2: 2N HBr / 1 h
View Scheme
参考文献
Andreani; Rambaldi; Bonazzi; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 3 p. 219 - 222
