4-硝基苯甲酰甲基硫氰酸酯合成路线 (共 11 条)
反应条件
pyridinium tribromide in acetonitrile T=0 - 20°C; 2 h; regioselective reaction;
参考文献
Wu, Liqiang; Yang, Xiaojuan
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 6 p. 748 - 753
反应条件
1: ammonium thiocyanate With montmorillonite K10 clay in acetone T=20°C; 0.666667 h; 2: 2-bromo-4'-nitroacetophenone T=20°C; 0.00555556 h; Neat (no solvent)Grinding;
参考文献
Meshram; Thakur, Pramod B.; Madhu Babu; Bangade, Vikas M.
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1780 - 1785
反应条件
in acetonitrile T=45°C; 3 h;
参考文献
Rudolph; Theis; Hanke; Endermann; Johannsen; Geschke
Journal of Medicinal Chemistry, 2001 , vol. 44, # 4 p. 619 - 626
反应条件
β-cyclodextrin-silica nanocomposite linked by propyl spacer in water T=90°C; 0.5 h; Green chemistry;
参考文献
Kiasat, Ali Reza; Nazari, Simin
Journal of Inclusion Phenomena and Macrocyclic Chemistry, 2013 , vol. 77, # 1-4 p. 429 - 438
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile T=20°C; 0.833333 h; regioselective reaction;
参考文献
Wu, Dezhen; Yang, Xiaojuan; Wu, Liqiang
Journal of Chemical Sciences (Bangalore), 2012 , vol. 124, # 4 p. 901 - 905,5
反应条件
cis-1,4-bis(triphenylphosphonium)-2-butene peroxodisulfate; oxygen in methanol T=0°C; 1.33333 h;
参考文献
Badri, Rashid; Gorjizadeh, Maryam
Synthetic Communications, 2012 , vol. 42, # 14 p. 2058 - 2066
反应条件
in water; isopropyl alcohol T=20°C; 0.0666667 h;
参考文献
Bisogno, Fabricio R.; Cuetos, Anibal; Lavandera, Ivan; Gotor, Vicente
Green Chemistry, 2009 , vol. 11, # 4 p. 452 - 454
反应条件
in neat (no solvent) T=30°C; 4 h;
参考文献
Muthyala, Manoj Kumar; Choudhary, Sunita; Kumar, Anil
RSC Advances, 2014 , vol. 4, # 27 p. 14297 - 14303
反应条件
1: bromine / dichloromethane / 5 h / 20 °C 2: ethanol / 1 h / Reflux View Scheme
参考文献
Bulletin of the Korean Chemical Society, , vol. 33, # 1 p. 111 - 114
参考文献
Singh, S. P.; Sehgal, Subhash; Diwakar, P.; Vaid, R. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, p. 573 - 575