3,4,5-三甲氧基硫代苯甲酰胺合成路线 (共 5 条)
反应条件
diphosphorus pentasulfide; sodium hydroxide in water; benzene
参考文献
Otsuka Pharmaceutical Co., Ltd.
Patent: US5643932 A1, 1997 ;
参考文献
Kowa Co., Ltd.
Patent: US6472386 B1, 2002 ;
反应条件
1: hydroxylamine hydrochloride, sodium hydroxide / aq. ethanol; H2O / Ambient temperature
2: acetic anhydride / Heating
3: hydrogen sulphide gas, triethylamine, pyridine / Ambient temperature
View Scheme
参考文献
Khadse, B. G.; Lokhande, S. R.; Bhamaria, R. P.; Prabhu, S. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 856 - 860
反应条件
pyridine; hydrogen sulfide; triethylamine
Ambient temperature;
参考文献
Khadse, B. G.; Lokhande, S. R.; Bhamaria, R. P.; Prabhu, S. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 856 - 860
反应条件
1: acetic anhydride / Heating
2: hydrogen sulphide gas, triethylamine, pyridine / Ambient temperature
View Scheme
参考文献
Khadse, B. G.; Lokhande, S. R.; Bhamaria, R. P.; Prabhu, S. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 856 - 860