1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.25 h / 0 °C 1.2: 0.5 h / 20 °C 2.1: [(R,R)-N,N-bis-(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediamino-Co(III)-acetate] / water / 61 h / 0 - 20 °C / |Resolution of racemate 3.1: methanol / 2 h / 20 °C 4.1: hydrogenchloride / methanol / 1 h / |Reflux View Scheme
参考文献
Organic Process Research and Development, , vol. 2, # 6 p. 422 - 424
Musser, John H.; Kubrak, Dennis M.; Bender, Reinhold H. W.; Kreft, Anthony F.; Nielsen, Susan T.; et al.
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