2,3,4-三羟基苯甲酸合成路线 （共 43 条）
反应条件
hydrogenchloride T=130°C; pH=1.36; Activation energyKinetics; Further Variations:TemperaturespH-values;
参考文献
Li, Jun; Brill, Thomas B.
Journal of Physical Chemistry A, 2003 , vol. 107, # 15 p. 2667 - 2673
参考文献
Berthoud; Porret
Journal de Chimie Physique et de Physico-Chimie Biologique, 1933 , vol. 30, p. 453,462
反应条件
zinc(II) chloride; trichlorophosphate T=70°C; Friedel-Crafts reaction; 2.5 h;
参考文献
Wu, Jianlong; Hu, Xuesen; Ma, Lin
Journal of Enzyme Inhibition and Medicinal Chemistry, 2011 , vol. 26, # 3 p. 449 - 452
参考文献
Pfeiffer; Breitbach; Scholl
Journal fuer Praktische Chemie (Leipzig), 1940 , vol. <2> 154, p. 157,195
反应条件
1: acetone; aq. NaOH solution / unter Ausschluss von Luft 2: quinoline; copper oxide-chromium oxide catalyst 3: acetone; potassium carbonate 4: 220 °C 5: aq. NaOH solution; aqueous potassium peroxo disulfate solution / Erwaermen des Reaktionsprodukts in Methanol mit Dimethylsulfat und wss. Kalilauge View Scheme
参考文献
Baker; Savage
Journal of the Chemical Society, 1938 , p. 1602,1605
反应条件
zinc(II) chloride; trichlorophosphate T=70°C; Friedel-Crafts reaction; 2.5 h;
参考文献
Wu, Jianlong; Hu, Xuesen; Ma, Lin
Journal of Enzyme Inhibition and Medicinal Chemistry, 2011 , vol. 26, # 3 p. 449 - 452
反应条件
1: NaOH-solution 2: chloroform; phosphorus pentachloride 3: aluminium chloride / Verseifen des Reaktionsproduktes mit verd. Natronlauge in Aceton im Wasserstoffstrom View Scheme
参考文献
Fischer,E.; Rapaport
Chemische Berichte, 1913 , vol. 46, p. 2394
反应条件
1: acetone; aq. NaOH solution / unter Ausschluss von Luft
2: quinoline; copper oxide-chromium oxide catalyst
3: aq. NaOH solution; aqueous potassium peroxo disulfate solution / Erwaermen des nach Ansaeuern geloesten Reaktionsprodukts mit wss. Salzsaeure
4: methanol; aqueous KOH-solution
View Scheme
参考文献
Baker; Savage
Journal of the Chemical Society, 1938 , p. 1602,1605
反应条件
1: aqueous methanol. NaOH-solution
2: aq. NaOH solution; aqueous potassium peroxo disulfate
3: acetone; aqueous KOH-solution
View Scheme
参考文献
Baker; Savage
Journal of the Chemical Society, 1938 , p. 1602,1605
反应条件
in Gegenwart eines Kondensationsmittels;
参考文献
Russell; Butler
Journal of the American Chemical Society, 1949 , vol. 71, p. 3663
