1: p-bromophenyl bromide With 2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran T=-80°C; Inert atmosphere; 2: carbon dioxide in tetrahydrofuran T=-75 - -20°C; 3: With sulfuric acid in tetrahydrofuran; water
参考文献
Lulinski, Sergiusz; Serwatowski, Janusz; Szczerbinska, Magdalena
European Journal of Organic Chemistry, 2008 , # 10 p. 1797 - 1801
1: 1,2,4-tribromo-benzene With isopropylmagnesium chloride in tetrahydrofuran T=-40°C; Grignard reaction; 2 h; 2: carbon dioxide in tetrahydrofuran T=-40°C; 1 h; Further stages. Title compound not separated from byproducts.;
