1: in diethyl ether
T=0 - 23°C; 3 h; Inert atmosphere;
2: With tert-butylhypochlorite in tetrachloromethane
T=23°C; 1 h; Inert atmosphere;
参考文献
Powers, David C.; Lee, Eunsung; Ariafard, Alireza; Sanford, Melanie S.; Yates, Brian F.; Canty, Allan J.; Ritter, Tobias
Journal of the American Chemical Society, 2012 , vol. 134, # 29 p. 12002 - 12009