2-苯基吡唑并[5,1-a]异喹啉合成路线 （共 17 条）
反应条件
tris(4-methoxyphenyl)-phosphine; silver benzoate; palladium (II) bromide in 1,4-dioxane
T=125°C; 16 h; Inert atmosphere;
参考文献
Mousseau, James J.; Bull, James A.; Ladd, Carolyn L.; Fortier, Angelique; Sustac Roman, Daniela; Charette, Andre B.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8243 - 8261
反应条件
potassium acetate; copper diacetate in 1,4-dioxane
T=120°C; 24 h; Sealed tube;
参考文献
Ling, Lin; Chen, Jingqing; Song, Jiahui; Zhang, Yuhai; Li, Xinqian; Song, Lijuan; Shi, Feng; Li, Yuxue; Wu, Chunrui
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3894 - 3902
反应条件
O-(2,4,6-trimethylbenzenesulfonyl)hydroxylamine in chloroform
T=25°C; 1 h;
参考文献
Gnichtel, Horst; Moeller, Bernd
Liebigs Annalen der Chemie, 1981 , # 10 p. 1751 - 1759
反应条件
silver trifluoromethanesulfonate in 1,2-dichloro-ethane
2 h; Reflux; chemoselective reaction;
参考文献
Xu, Su-Xia; Hao, Lu; Wang, Tao; Ding, Zong-Cang; Zhan, Zhuang-Ping
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 2 p. 294 - 298
反应条件
potassium carbonate in N,N-dimethyl-formamide
Ambient temperature;
参考文献
Tsuchiya, Takashi; Sashida, Haruki; Konoshita, Ari
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4568 - 4572
反应条件
manganese(IV) oxide in benzene
96 h; Heating;
参考文献
Toja; Omodei-Sale; Cattaneo; Galliani
European Journal of Medicinal Chemistry, 1982 , vol. 17, # 3 p. 223 - 227
反应条件
1: 20.2 g / p-toluenesulfonic acid / benzene / 1 h / Heating
2: 18.3 g / potassium t-butoxide / 2-methyl-propan-2-ol / 5 h / Heating
3: 87 percent / 98percent H2SO4 / ethanol / 11 h / Heating
4: 46 percent / MnO2 / benzene / 96 h / Heating
View Scheme
参考文献
Toja; Omodei-Sale; Cattaneo; Galliani
European Journal of Medicinal Chemistry, 1982 , vol. 17, # 3 p. 223 - 227
反应条件
1: 20.2 g / p-toluenesulfonic acid / benzene / 1 h / Heating
2: 18.3 g / potassium t-butoxide / 2-methyl-propan-2-ol / 5 h / Heating
3: 87 percent / 98percent H2SO4 / ethanol / 11 h / Heating
4: 46 percent / MnO2 / benzene / 96 h / Heating
View Scheme
参考文献
Toja; Omodei-Sale; Cattaneo; Galliani
European Journal of Medicinal Chemistry, 1982 , vol. 17, # 3 p. 223 - 227
反应条件
1: 18.3 g / potassium t-butoxide / 2-methyl-propan-2-ol / 5 h / Heating
2: 87 percent / 98percent H2SO4 / ethanol / 11 h / Heating
3: 46 percent / MnO2 / benzene / 96 h / Heating
View Scheme
参考文献
Toja; Omodei-Sale; Cattaneo; Galliani
European Journal of Medicinal Chemistry, 1982 , vol. 17, # 3 p. 223 - 227
反应条件
1: 87 percent / 98percent H2SO4 / ethanol / 11 h / Heating
2: 46 percent / MnO2 / benzene / 96 h / Heating
View Scheme
参考文献
Toja; Omodei-Sale; Cattaneo; Galliani
European Journal of Medicinal Chemistry, 1982 , vol. 17, # 3 p. 223 - 227
