(3E)-2-氯-3-(羟基亚甲基)-5-(2-甲基-2-丙基)-1-环己烯-1-甲醛合成路线 (共 1 条)
反应条件
1: N,N-dimethyl-formamide With trichlorophosphate
T=0 - 5°C; 0.25 h; Inert atmosphere;
2: 4-(1,1-dimethylethyl)cyclohexanone T=0 - 80°C; 3 h;
参考文献
ECOLE NORMALE SUPERIEURE DE LYON; Bretonniere, Yann; Andraud, Chantal; Buron, Wissam
Patent: US2013/123508 A1, 2013 ;
Location in patent: Paragraph 0164-0166 ;