2,2,5-三甲基-4-苯基-3-氮杂己烷-3-氮氧自由基合成路线 （共 9 条）
反应条件
sodium tetrahydroborate; (salen)Mn in ethanol; benzene T=20°C; 15 h;
参考文献
Lee, Sang-Min; Chen, Haimei; Dettmer, Christine M.; O'Halloran, Thomas V.; Nguyen, Sonbinh T.
Journal of the American Chemical Society, 2007 , vol. 129, # 49 p. 15096 - 15097
反应条件
lead dioxide 1.) toluene, 5 min., irrad., 2.) toluene, from -78 deg C to RT, 1 h; Yield givenMultistep reaction;
参考文献
Benoit, Didier; Chaplinski, Vladimir; Braslau, Rebecca; Hawker, Craig J.
Journal of the American Chemical Society, 1999 , vol. 121, # 16 p. 3904 - 3920
反应条件
in various solvent(s) T=23.84°C; Kinetics; Further Variations:Temperatures;
参考文献
Sobek; Martschke; Fischer
Journal of the American Chemical Society, 2001 , vol. 123, # 12 p. 2849 - 2857
参考文献
Chen,J.Y. et al.
Journal of the American Chemical Society, 1976 , vol. 98, p. 6150 - 6159
反应条件
ammonium hydroxide; copper diacetate; air
1.) THF, Et2O, RT, 12 h, 2.) THF, Et2O, MeOH, 10 min; Yield givenMultistep reaction;
参考文献
Benoit, Didier; Chaplinski, Vladimir; Braslau, Rebecca; Hawker, Craig J.
Journal of the American Chemical Society, 1999 , vol. 121, # 16 p. 3904 - 3920
反应条件
in diethyl ether
T=20°C; 0.166667 h; Title compound not separated from byproducts;
参考文献
Novakov; Feierman; Cederbaum; Stoyanovsky
Chemical Research in Toxicology, 2001 , vol. 14, # 9 p. 1239 - 1246
反应条件
in benzene
T=55°C; 0.05 h;
参考文献
Abe, Yukino; Seno, Shin-ya; Sakakibara, Kazuhisa; Hirota, Minoru
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 6 p. 897 - 903
反应条件
in various solvent(s)
T=393°C; Kinetics;
参考文献
Sobek; Martschke; Fischer
Journal of the American Chemical Society, 2001 , vol. 123, # 12 p. 2849 - 2857
反应条件
T=130°C; Activation energy;
参考文献
Molawi, Kian; Schulte, Tobias; Siegenthaler, Kai Oliver; Wetter, Christian; Studer, Armido
Chemistry - A European Journal, 2005 , vol. 11, # 8 p. 2335 - 2350
