2,6-二甲基-4-氧代-2-环己烯-1-羧酸乙酯合成路线 （共 4 条）
反应条件
sodium hydroxide anschliessend mit wss. H2SO4;
参考文献
Ciocca; Scattola
Gazzetta Chimica Italiana, 1936 , vol. 66, p. 394,397
Full Text Show Details
Horning; Denekas; Field
Journal of Organic Chemistry, 1944 , vol. 9, p. 547,549
Organic Syntheses, 1955 , vol. Coll. Vol. III, p. 317
反应条件
carbon disulfide; bromine
1) -10 deg C; 2) RT,;
参考文献
Bhattacharya, Kalyan K.; Pal, Panchanan; Ghosh, Kalpana; Sen, P. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 3 p. 191 - 194
反应条件
1: aq.-ethanolic NaOH / anschliessend mit wss. H2SO4
View Scheme
参考文献
Ciocca; Scattola
Gazzetta Chimica Italiana, 1936 , vol. 66, p. 394,397
反应条件
1: sodium amide; liquid ammonia / Erwaermen des nach Zusatz von Aether vom Ammoniak befreiten Reaktionsgemisches mit Aethyljodid in Aether und Toluol
2: aq.-ethanolic NaOH / Ansaeuern mit wss. H2SO4 und erneuten Kochen
View Scheme
参考文献
Horning; Horning; Walker
Journal of the American Chemical Society, 1949 , vol. 71, p. 169
