N-甲酸基-2-甲氧基哌啶合成路线 （共 6 条）
反应条件
1: 73 percent / AlCl3 / CH2Cl2 / 20 h / Ambient temperature 2: 1.) aq. NaOH, 2.) aq. HCl / 1) reflux, 20 h; 3) 100 deg C, 1 mmHg View Scheme
参考文献
Eberson, Lennart; Malmberg, Mats; Nyberg, Klas
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 6 p. 555 - 566
反应条件
tetraethylammonium p-toluenesulfonate
Electrochemical reaction;
参考文献
Moriyama, Noriaki; Matsumura, Yoshihiro; Kuriyama, Masami; Onomura, Osamu
Tetrahedron Asymmetry, 2009 , vol. 20, # 23 p. 2677 - 2687
反应条件
aluminium trichloride in dichloromethane
20 h; Ambient temperature;
参考文献
Eberson, Lennart; Malmberg, Mats; Nyberg, Klas
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 6 p. 555 - 566
反应条件
1: 71 percent / AlCl3 / CH2Cl2 / 2.5 h / Ambient temperature
2: 1.) aq. NaOH, 2.) aq. HCl / 1) room temperature, 24 h; 3) 100 deg C, in vacuo
View Scheme
参考文献
Eberson, Lennart; Malmberg, Mats; Nyberg, Klas
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 6 p. 555 - 566
反应条件
1: 73 percent / AlCl3 / CH2Cl2 / 20 h / Ambient temperature
2: 78 percent / aq. NaOH / 20 h / Ambient temperature
View Scheme
参考文献
Eberson, Lennart; Malmberg, Mats; Nyberg, Klas
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 6 p. 555 - 566
