alpha,alpha-二氯苯乙酸合成路线 （共 6 条）
反应条件
lithium hydroxide in water; isopropyl alcohol
T=-7°C; 0.25 h;
参考文献
Benedetti, Miriam; Forti, Luca; Ghelfi, Franco; Pagnoni, Ugo Maria; Ronzoni, Roberto
Tetrahedron, 1997 , vol. 53, # 41 p. 14031 - 14042
反应条件
tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
electrochemical reduction;
参考文献
Gisselbrecht, Jean-Paul; Lund, Henning
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1985 , vol. 39, # 10 p. 823 - 828
参考文献
Radziszewski
Chemische Berichte, 1869 , vol. 2, p. 209
Chemische Berichte, 1870 , vol. 3, p. 648
参考文献
Claisen
Chemische Berichte, 1879 , vol. 12, p. 633
Chemische Berichte, 1877 , vol. 10, p. 1663
反应条件
1: AlCl3
2: bei der Oxydation
View Scheme
参考文献
Combes
Bulletin de la Societe Chimique de France, 1884 , vol. <2> 41, p. 382
Annales de Chimie (Cachan, France), 1887 , vol. <6> 12, p. 271
反应条件
tetrachloromethane; sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
1.) room temperature, 20 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lauritzen, Stein Erik; Roemming, Christian; Skatteboel, Lars
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1981 , vol. 35, # 4 p. 263 - 268
