2,4,6-三甲氧基苯乙醇合成路线 （共 8 条）
反应条件
sodium formate; N-(2-amino-ethyl)-4-methyl-benzenesulphonamide; [{(η5-C5Me5)IrCl}2(μ-Cl)2] T=80°C; 1.5 h;
参考文献
Wu, Xiaofeng; Liu, Jianke; Li, Xiaohong; Zanotti-Gerosa, Antonio; Hancock, Fred; Vinci, Daniele; Ruan, Jiwu; Xiao, Jianliang
Angewandte Chemie - International Edition, 2006 , vol. 45, # 40 p. 6718 - 6722
反应条件
Co(III)W in water; acetic acid 0.5 h; Ambient temperature; Product distribution;
参考文献
Tetrahedron, , vol. 53, # 36 p. 12287 - 12298
参考文献
Justus Liebigs Annalen der Chemie, , vol. 451, p. 222
反应条件
1: With toluene-4-sulfonic acid; thiourea in acetonitrile 2: With sodium hydroxide Further stages.;
参考文献
Vetter, Stefan
Synthetic Communications, 1998 , vol. 28, # 17 p. 3219 - 3223
反应条件
1: 98 percent / HSiEt3; CF3COOH / CH2Cl2 / -78 - 20 °C 2: 77 percent / SnCl4 / CH2Cl2 / -10 °C 3: 80 percent / BBr3 / CH2Cl2 / -78 - 20 °C View Scheme
参考文献
Roelens, Frederik; Heldring, Nina; Dhooge, Willem; Bengtsson, Martin; Comhaire, Frank; Gustafsson, Jan-Ake; Treuter, Eckardt; De Keukeleire, Denis
Journal of Medicinal Chemistry, 2006 , vol. 49, # 25 p. 7357 - 7365
反应条件
K2OsO2(OH)4; chloramine-T in water; tert-butyl alcohol 0.416667 h; chemoselective reaction;
参考文献
Devari, Shekaraiah; Deshidi, Ramesh; Kumar, Manjeet; Kumar, Arvind; Sharma, Simmi; Rizvi, Masood; Kushwaha, Manoj; Gupta, Ajai Prakash; Shah, Bhahwal Ali
Tetrahedron Letters, 2013 , vol. 54, # 48 p. 6407 - 6410
反应条件
tert.-butylhydroperoxide; copper(ll) bromide in water; dimethyl sulfoxide T=20°C; 8.5 h; Inert atmosphere;
参考文献
Das, Rima; Chakraborty, Debashis
Applied Organometallic Chemistry, 2011 , vol. 25, # 6 p. 437 - 442
反应条件
pyridine; 1,1,1,3,3,3-hexamethyl-disilazane
参考文献
Midgley,J.M. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 1384 - 1385
