3,5-二甲氧基-4-甲基苯甲酸合成路线 （共 16 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=-10°C; Inert atmosphereReflux;
参考文献
Harmata, Michael; Ying, Weijiang; Barnes, Charles L.
Tetrahedron Letters, 2009 , vol. 50, # 20 p. 2326 - 2328
参考文献
Spirogen Limited
Patent: US2003/120069 A1, 2003 ;
反应条件
sulfuric acid
5 h; Heating / reflux;
参考文献
Spirogen Limited
Patent: EP1193270 A2, 2002 ;
Location in patent: Page 78, 127 ;
反应条件
potassium carbonate; acetone
参考文献
King; Grundon
Journal of the Chemical Society, 1949 , p. 3348
Journal of the Chemical Society, 1950 , p. 3547
参考文献
Fujikawa; Yurugi
Yakugaku Zasshi, 1943 , vol. 63, p. 341
Chem.Abstr., 1951 , p. 5128
反应条件
1: SOCl2 / benzene
2: diethyl ether
3: aq. NH3, AgNO3 / dioxane
4: LiAlH4 / diethyl ether; benzene
View Scheme
参考文献
Benington,F. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 2066 - 2067
