4-氯-5-甲基-2-(甲基硫代)嘧啶合成路线 (共 3 条)
反应条件
ammonium hydroxide 2 h; Heating;
参考文献
Youssef, Mohamed M.; Youssef, Ayman M. S.
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 1 p. 67 - 81
反应条件
trichlorophosphate
T=120°C; 2 h;
参考文献
BANYU PHARMACEUTICAL CO., LTD.
Patent: EP1754706 A1, 2007 ;
Location in patent: Page/Page column 94 ;
反应条件
1: 90 percent / KOH / ethanol / 2 h / Heating
2: 60 percent / POCl3 / dioxane / 2 h / Heating
View Scheme
参考文献
Youssef, Mohamed M.; Youssef, Ayman M. S.
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 1 p. 67 - 81