Bair, Kenneth W.; Tuttle, Richard L.; Knick, Vincent C.; Cory, Michael; McKee, David D.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 9 p. 2385 - 2393
1: 77 percent / 0.58 h / 210 °C
2: B2H6 / tetrahydrofuran / 26 h / Ambient temperature
View Scheme
参考文献
Bair, Kenneth W.; Tuttle, Richard L.; Knick, Vincent C.; Cory, Michael; McKee, David D.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 9 p. 2385 - 2393
1: KOH / ethanol; H2O / Heating
2: 77 percent / 0.58 h / 210 °C
3: B2H6 / tetrahydrofuran / 26 h / Ambient temperature
View Scheme
参考文献
Bair, Kenneth W.; Tuttle, Richard L.; Knick, Vincent C.; Cory, Michael; McKee, David D.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 9 p. 2385 - 2393
N-bromosuccinmide; triphenylphosphine in dichloromethane
T=-10 - 20°C; 3 h;
参考文献
Nishimura, Tomoki; Xu, Su-Ying; Jiang, Yun-Bao; Fossey, John S.; Sakurai, Kazuo; Bull, Steven D.; James, Tony D.
Chemical Communications, 2013 , vol. 49, # 5 p. 478 - 480
