N-bromosuccinmide; triphenylphosphine in dichloromethane
T=-10 - 20°C; 3 h;
参考文献
Nishimura, Tomoki; Xu, Su-Ying; Jiang, Yun-Bao; Fossey, John S.; Sakurai, Kazuo; Bull, Steven D.; James, Tony D.
Chemical Communications, 2013 , vol. 49, # 5 p. 478 - 480
1: sodium tetrahydroborate; CoCl2.6H2O / tetrahydrofuran; methanol / 2 h / 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C
3: N-bromosuccinmide; triphenylphosphine / dichloromethane / 3 h / -10 - 20 °C
View Scheme
参考文献
Nishimura, Tomoki; Xu, Su-Ying; Jiang, Yun-Bao; Fossey, John S.; Sakurai, Kazuo; Bull, Steven D.; James, Tony D.
Chemical Communications, 2013 , vol. 49, # 5 p. 478 - 480
