1: With benzo[1,3,2]dioxaborole; rhodium complex 2 in toluene T=20°C; Addition; Hydroboration; 2 h; 2: With sodium hydroxide; water; dihydrogen peroxide in toluene T=20°C; Oxidation; 2 h; Title compound not separated from byproducts;
参考文献
Demay, Steandphane; Volant, Florence; Knochel, Paul
Angewandte Chemie - International Edition, 2001 , vol. 40, # 7 p. 1235 - 1238
1: With benzo[1,3,2]dioxaborole; rhodium complex 2 in toluene T=20°C; Addition; Hydroboration; 2 h; 2: With sodium hydroxide; water; dihydrogen peroxide in toluene T=20°C; Oxidation; 2 h; Title compound not separated from byproducts;
参考文献
Demay, Steandphane; Volant, Florence; Knochel, Paul
Angewandte Chemie - International Edition, 2001 , vol. 40, # 7 p. 1235 - 1238
in acetic acid T=118°C; 2 h; Further byproducts given;
参考文献
Norman, Julie A.; Thomas, C. Barry; Burrow, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1087 - 1094
in acetic acid T=118°C; 2 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Norman, Julie A.; Thomas, C. Barry; Burrow, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1087 - 1094