Zn; NH4Cl in tetrahydrofuran; water
air; addn. of organotin (1 equiv.) to suspension of Zn-powder (2 equivs.) in satd. soln. of NH4Cl in H2O:THF, dropwise addn. of benzyl bromide (2 equivs.) with rate maintaining gentle reflux, stirring with cooling toroom temp. for 30 min; sepn. of org. layer, evapn., distillation (vac.); elem. anal.;
参考文献
Marton, Daniele; Russo, Umberto; Stivanello, Diego; Tagliavini, Giuseppe; Ganis, Paolo; Valle, Giovanni Carlo
Organometallics, 1996 , vol. 15, # 6 p. 1645 - 1650
Zhukauskaite, L. N.; Tsybusov, A. P.; Gendenshtein, E. I.; Stankevichyus, A. P.; Tseplene, V. S.; Lubas, A. A.
Pharmaceutical Chemistry Journal, 1981 , vol. 15, # 6 p. 391 - 396
Khimiko-Farmatsevticheskii Zhurnal, 1981 , vol. 15, # 6 p. 43 - 48
