反应条件
1: 1.) 3-chloroperoxybenzoic acid, 2.) NaOH / 1.) CHCl3, room temperature, 20 min, 2.) reflux, 1.5 h 2: 73 percent / H2 / Pd-C / ethyl acetate / 2 h / 760 Torr / Ambient temperature 3: 80 percent / -105 deg C -> room temperature, 1.5 h 4: 84 percent / W-2 Raney nickel / ethanol / 1 h / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 18, # 10 p. 1035 - 1042
