2-甲基-1-苯基-1-丙醇合成路线 （共 136 条）
反应条件
benzoic acid anhydride; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 12 h; Title compound not separated from byproducts.;
参考文献
Shiina, Isamu; Nakata, Kenya
Tetrahedron Letters, 2007 , vol. 48, # 47 p. 8314 - 8317
反应条件
benzoic acid anhydride; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 12 h; Title compound not separated from byproducts.;
参考文献
Shiina, Isamu; Nakata, Kenya
Tetrahedron Letters, 2007 , vol. 48, # 47 p. 8314 - 8317
反应条件
Birman's catalyst; trimethylacetic anhydride; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 12 h; optical yield given as percent eeenantioselective reaction;
参考文献
Shiina, Isamu; Nakata, Kenya; Sugimoto, Masuhiro; Onda, Yu-Suke; Iizumi, Takashi; Ono, Keisuke
Heterocycles, 2009 , vol. 77, # 2 p. 801 - 810
参考文献
Ruble; Latham; Fu
Journal of the American Chemical Society, 1997 , vol. 119, # 6 p. 1492 - 1493
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Vedejs, Edwin; Daugulis, Olafs
Journal of the American Chemical Society, 1999 , vol. 121, # 24 p. 5813 - 5814
反应条件
1: 73 percent / copper(II) triflate 2: 90 percent / 1,4-dicyanobenzene, biphenyl, 2,4,6-trimethylpyridine / acetonitrile / 10 °C / Irradiation View Scheme
参考文献
Arnold, Donald R.; Mines, Shelley A.
Canadian Journal of Chemistry, 1989 , vol. 67, p. 689 - 698
反应条件
potassium hydrogensulfate T=120 - 130°C; 3 h; Title compound not separated from byproducts;
参考文献
Knorr, Rudolf; Lattke, Ernst
Chemische Berichte, 1981 , vol. 114, # 6 p. 2116 - 2131
反应条件
C4H7N2O3S(1+)*HO4S(1-) T=20°C; 0.166667 h; Neat (no solvent);
参考文献
Khaligh, Nader Ghaffari
Journal of Molecular Catalysis A: Chemical, 2011 , vol. 349, # 1-2 p. 63 - 70
反应条件
C12H7N2O7V(1-)*H(1+); oxygen in ethanol T=120°C; P=7500.75 Torr; 12 h; Autoclave;
参考文献
Kodama, Shintaro; Ueta, Yukihiro; Yoshida, Jun; Nomoto, Akihiro; Yano, Shigenobu; Ueshima, Michio; Ogawa, Akiya
Dalton Transactions, 2009 , # 44 p. 9708 - 9711
反应条件
1: With MnIII(L-5-t-Bu)(Cl); 1-butyl-2,6-dimethyl-pyridinium; bromide in dichloromethane; water T=20°C; 2: With [bis(acetoxy)iodo]benzene in dichloromethane; water T=20°C; 0.1 h;
参考文献
Zhang, Yuecheng; Zhou, Qiao; Ma, Wenchan; Zhao, Jiquan
Catalysis Communications, 2014 , vol. 45, p. 114 - 117
反应条件
1: 1-hydroxy-2-(1-methyl)-propylbenzene With zinc(II) chloride; lithium tert-butylate in tetrahydrofuran 2 h; RefluxInert atmosphere; 2: (S)-pentafluorophenyl 2-phenylbutanoate in tetrahydrofuran T=20°C; 12 h; Inert atmosphere;
参考文献
Coulbeck, Elliot; Eames, Jason
Tetrahedron Letters, 2009 , vol. 50, # 31 p. 4449 - 4451
