2-甲基-1-苯基-1-丙醇合成路线 （共 136 条）
反应条件
nickel monoaluminide in water 2 h; Heating; Title compound not separated from byproducts.;
参考文献
Chemical Communications, , # 4 p. 514 - 515
反应条件
1: isopropylmagnesium chloride lithium chloride complex With 2,2,6,6-tetramethyl-piperidine in tetrahydrofuran Inert atmosphere; 2: benzaldehyde Inert atmosphere;
参考文献
Organic Letters, , vol. 12, # 9 p. 1984 - 1987
反应条件
in toluene 5 h; Ambient temperature;
参考文献
Boudin, Alain; Cerveau, Genevieve; Chuit, Claude; Corriu, Robert J.P.; Reye, Catherine
Tetrahedron, 1989 , vol. 45, # 1 p. 171 - 180
反应条件
water-d2; uranium(IV) hydrochloride; lithium in THF-d8 (tetrahydrofuran-d8) T=20°C; 12 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 38, # 37 p. 6591 - 6594
反应条件
1: phenylboronic acid neopentylglycol ester With bis(1,5-cyclooctadiene)nickel (0); Ipr.HCl; cesium fluoride in 1,4-dioxane; toluene T=20°C; 0.5 h; Inert atmosphere; 2: 2-methyl-propan-1-ol With chlorobenzene in 1,4-dioxane; toluene T=60°C; 10 h; Inert atmosphere;
参考文献
Maekawa, Takehisa; Sekizawa, Hiromi; Itami, Kenichiro
Angewandte Chemie - International Edition, 2011 , vol. 50, # 31 p. 7022 - 7026
反应条件
lithium; naphthalene 1) THF, -78 deg C, 1 h, 2) THF, -78 to 20 deg C, 5 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 33, # 38 p. 5597 - 5600
反应条件
1: phenylboronic acid neopentylglycol ester With bis(1,5-cyclooctadiene)nickel (0); Ipr.HCl; cesium fluoride in 1,4-dioxane; toluene T=20°C; 0.5 h; Inert atmosphere; 2: 2-methyl-propan-1-ol With chlorobenzene in 1,4-dioxane; toluene T=60°C; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 31 p. 7022 - 7026
参考文献
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 44, p. 1387
Chem. Zentralbl., , vol. 84, # I p. 1010
Helvetica Chimica Acta, , vol. 65, # 7 p. 2061 - 2070
反应条件
1: morpholine / acetic acid; H2O / Heating 2: baker's yeast Saccharomyces cerevisiae / H2O / 144 h / 30 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 12, # 6 p. 847 - 852
反应条件
1: naphthalene; Li / tetrahydrofuran / 0.58 h / -30 °C 2: 38 percent / tetrahydrofuran / 3 h / -30 - 0 °C View Scheme
参考文献
Tetrahedron, , vol. 56, # 8 p. 1135 - 1138
