N,N-二甲基苯甲酰胺合成路线 (共 319 条)
反应条件
lithium 9-BBN hydride in tetrahydrofuran T=15°C; 24 h; also with other amides; Product distribution;
参考文献
Brown, Herbert C.; Mathew, C. Poonoose; Pyun, Chongsuh; Son, Jong Chan; Yoon, Nung Min
Journal of Organic Chemistry, 1984 , vol. 49, # 17 p. 3091 - 3097
反应条件
water; sodium acetate; trichlorophosphate Yield given. Multistep reaction;
参考文献
Alexandrou; Rekka; Demopoulos
Synthetic Communications, 1992 , vol. 22, # 5 p. 761 - 766
参考文献
v. Braun
Chemische Berichte, 1904 , vol. 37, p. 2816
反应条件
trichlorophosphate 1.) 5 min, 100 deg C, 2.) CH3CN, 30 min, reflux; Yield given. Multistep reaction;
参考文献
Harris, Roger L.N.
Synthesis, 1980 , # 10 p. 841 - 842
反应条件
T=100°C; P=0.008 - 0.8 Torr; radio-frequency discharge; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Yajima, Tatsuhiko; Tsuchiya, Atsuhiko; Tezuka, Meguru
Tetrahedron Letters, 1987 , vol. 28, # 36 p. 4177 - 4178
反应条件
ammonia; ammonium chloride T=-33°C; 0.166667 h;
参考文献
Journal of Organic Chemistry, , vol. 51, # 25 p. 4983 - 4987
反应条件
(.eta.5-pentamethylcyclopentadienyl)(.eta.6-hexamethylbenzene)rhodium(I) in further solvent(s) byproducts: H2; as solvent C6H5C(O)NEt2; at 150°C for 0.5 h; as mixt. of isomers;
参考文献
Journal of the American Chemical Society, , vol. 122, # 51 p. 12868 - 12869
反应条件
NiI2; samarium diiodide in tetrahydrofuran T=0°C; Barbier reaction; 0.5 h;
参考文献
Kang, Han-Young; Song, Sang-Eun
Tetrahedron Letters, 2000 , vol. 41, # 6 p. 937 - 939
反应条件
man giesst dann in Wasser;
参考文献
van Romburgh
Recueil des Travaux Chimiques des Pays-Bas, 1885 , vol. 4, p. 389
反应条件
1: 4-Methylpyridine With n-butyllithium; 2-(dimethylamino)-ethanol in hexane T=0°C; 1 h; 2: N,N-dimethyl benzamide in tetrahydrofuran; hexane T=-78°C; 1 h; Further stages.;
参考文献
Kaminski, Thomas; Gros, Philippe; Fort, Yves
European Journal of Organic Chemistry, 2003 , # 19 p. 3855 - 3860