N,N-二甲基苯甲酰胺合成路线 （共 319 条）
反应条件
1: 1) POCl3 / 2) CH2Cl2, 10-20 degC View Scheme
参考文献
Boyd, Gerhard V.; Lindley, Peter F.; Nicolaou, George A.
Journal of the Chemical Society, Chemical Communications, 1984 , # 16 p. 1105 - 1107
反应条件
1: With Bu3SnLi in tetrahydrofuran 2: With water-d2 in tetrahydrofuran
参考文献
Paleo, M. Rita; Calaza, M. Isabel; Grana, Paula; Sardina, F. Javier
Organic Letters, 2004 , vol. 6, # 6 p. 1061 - 1063
反应条件
1: phenylacetylene With n-butyllithium in diethyl ether T=-78°C; 2: N,N-dimethyl benzamide in diethyl ether T=-78 - 4°C; 3 h;
参考文献
Trost, Barry M.; Bertogg, Andreas
Organic Letters, 2009 , vol. 11, # 3 p. 511 - 513
反应条件
in tetrahydrofuran T=-78 - 25°C; 0.5 h;
参考文献
Katritzky, Alan R.; Sengupta, Saumitra
Tetrahedron Letters, 1987 , vol. 28, # 17 p. 1847 - 1850
反应条件
1: 1.) samarium(III) trifluoromethanesulfonate, s-butyllithium, hexamethylphosphoric triamide / 1.) THF, cyclohexane, room temperature, 1 h, 2.) THF, cyclohexane, room temperature, 1 h 2: 1.) samarium(III) trifluoromethanesulfonate, s-butyllithium, hexamethylphosphoric triamide / 1.) THF, cyclohexane, room temperature, 1 h, 2.) THF, cyclohexane, room temperature, 1 h View Scheme
参考文献
Fukuzawa, Shin-Ichi; Mutoh, Keisuke; Tsuchimoto, Teruhisa; Hiyama, Tamejiro
Journal of Organic Chemistry, 1996 , vol. 61, # 16 p. 5400 - 5405
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; sec.-butyllithium; Sm(OTf)3 1.) THF, cyclohexane, room temperature, 1 h, 2.) THF, cyclohexane, room temperature, 1 h; Yield given. Multistep reaction;
参考文献
Fukuzawa, Shin-Ichi; Mutoh, Keisuke; Tsuchimoto, Teruhisa; Hiyama, Tamejiro
Journal of Organic Chemistry, 1996 , vol. 61, # 16 p. 5400 - 5405
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 17, p. 193
反应条件
tetrapropylammonium perruthennate; Azobenzene in acetonitrile T=20°C; 0.0833333 h; Hg-cathode;
参考文献
Kistenbruegger, Lothar; Mischke, Peter; Voss, Juergen; Wiegand, Gabriele
Liebigs Annalen der Chemie, 1980 , # 3 p. 461 - 471
反应条件
[Re2(CO)10] in toluene T=180°C; 24 h;
参考文献
Sueki, Shunsuke; Guo, Yuanfang; Kanai, Motomu; Kuninobu, Yoichiro
Angewandte Chemie - International Edition, 2013 , vol. 52, # 45 p. 11879 - 11883
Angew. Chem., 2013 , p. 12095 - 12099
反应条件
2: LiAlH4 / tetrahydrofuran / 1 h / 0 °C 3: 26 percent / O2 / propionic acid / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 18 p. 2411 - 2412
