4,4'-二甲基二苯甲酮合成路线 （共 247 条）
反应条件
copper ferrite in neat (no solvent) T=80°C; Friedel-Crafts Acylation; 18 h;
参考文献
Parella, Ramarao; Naveen; Kumar, Amit; Babu, Srinivasarao Arulananda
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1738 - 1742
反应条件
quinoline; 1,10-phenanthroline; tris-(o-tolyl)phosphine; copper(I) bromide in 1-methyl-pyrrolidin-2-one; quinoline T=170°C; 16 h;
参考文献
Goossen, Lukas J.; Rudolphi, Felix; Oppel, Christoph; Rodriguez, Nuria
Angewandte Chemie - International Edition, 2008 , vol. 47, # 16 p. 3043 - 3045
反应条件
1: para-bromotoluene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: 4-methyl-benzaldehyde in tetrahydrofuran; hexane T=-78 - 20°C; 1 h; 3: With iodine; potassium carbonate in tert-butyl alcohol 7 h; Reflux;
参考文献
Ushijima, Sousuke; Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 5 p. 1436 - 1442
反应条件
tert.-butylhydroperoxide; bismuth(III)oxide in water; ethyl acetate 4 h; Reflux; Kinetics; Concentration; chemoselective reaction;
参考文献
Malik, Payal; Chakraborty, Debashis
Synthesis, 2010 , # 21 art. no. Z17610SS, p. 3736 - 3740
反应条件
NHC-Pd(II)-Im; sodium hydrogencarbonate in water T=50°C; 12 h; Inert atmosphere;
参考文献
Lin, Xiao-Fang; Li, Yao; Li, Shuang-Yan; Xiao, Zheng-Kang; Lu, Jian-Mei
Tetrahedron, 2012 , vol. 68, # 29 p. 5806 - 5809
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 3 h;
参考文献
Rao, Maddali L.N.; Venkatesh, Varadhachari; Banerjee, Debasis
Tetrahedron, 2007 , vol. 63, # 52 p. 12917 - 12926
反应条件
AlCl3, aluminium chloride in toluene T=-5 - 5°C;
参考文献
Wang, Lian-Jun; Li, Jie; Wang, Le-Yong
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 9 p. 3306 - 3310
反应条件
sodium periodate in tetrahydrofuran; water T=20°C; 0.116667 h;
参考文献
Basavaraju; Sharma, Siddharth; Maurya, Ram Awatar; Kim, Dong-Pyo
Angewandte Chemie - International Edition, 2013 , vol. 52, # 26 p. 6735 - 6738
Angew. Chem., 2013 , vol. 125, # 26 p. 6678
反应条件
hexaethyl distannane; triethyl phosphite; bis(η3-allyl-μ-chloropalladium(II)) in toluene T=111°C; 2 h;
参考文献
Journal of Organometallic Chemistry, , vol. 282, p. 421 - 426
反应条件
sodium methylate; tris(dibenzylideneacetone)dipalladium (0) in chloroform T=20°C; P=760 Torr; 3 h;
参考文献
Kang; Ryu; Choi
Synthetic Communications, 2001 , vol. 31, # 7 p. 1035 - 1039
